Separation of chlorinated hydrocarbons and organophosphorus, pyrethroid pesticides by silicagel fractionation chromatography and their simultaneous determination by GC-MS环境科学学报：英文版论文

【题名】：Separation of chlorinated hydrocarbons and organophosphorus, pyrethroid pesticides by silicagel fractionation chromatography and their simultaneous determination by GC-MS环境科学学报：英文版论文(Separation of chlorinated hydrocarbons and organophosphorus, pyrethroid pesticides by silicagel fractionation chromatography and their simultaneous determination by GC-MSHuanJingKeXueXueBao：YingWenBanLunWen)
【关键词】：碳氢化合物杀虫剂有机磷农药合成除虫菊酯分离技术
【keywords】：TanQingHuaHeWu ShaChongJi YouJiLinNongYao HeChengChuChongJuZuo FenLiJiShu
【作者】：WANGLi-gang,JIANGXin,WANGFang,BIANYong-rong,StephanForster,DieterMartens,      【来源】：知识词典
【期刊名称】：环境科学学报：英文版(HuanJingKeXueXueBao：YingWenBan)
【国际标准刊号】：1001-0742        【国内统一刊号】：11-2629/X
【作者单位】：[1]InstituteofSoilScience,ChineseAcademyofSciences,Nanjing210008,China. [2]InstituteofEcologicalChemistry,NationalResearchCenterforEnvironmentandHealth,Neuherberg85764,Germany([1]InstituteofSoilScience,ChineseAcademyofSciences,Nanjing210008,China. [2]InstituteofEcologicalChemistry,NationalResearchCenterforEnvironmentandHealth,Neuherberg85764,Germany)
【分类号】：X132      【页码】：-268-271      【出版年】：2004.2
        A silicagel fractionation procedure for environmental sample extracts, which separates chlorinated hydrocarbons(CHCs) and organophosphorus, pyrethroid pesticides into two groups for subsequent instrumental analysis, was developed in this study. This method was achieved by optimizing the fraction cut-off volume of elution and different solvents. Using fully activated silica gel and cut-off CHCs collection after 10ml 10% dichloromethane (DCM) in n-hexane passing through the column resulted in satisfactory separation of CHCs and organophosphorus, pyrethroid pesticides. This procedure had a higher reliability for CHCs than for organophosphorus, pyrethroid pesticides, because there is a relatively reliable recovery for CHCs. This approach is less expensive due to reducing sample pre-treatment time and solvent consumption.

Simultaneous Determination of Heroin, Amphetamine and their Basic Impurities and Adulterants Using Microemulsion Electrokinetic Chromatography - 中国化学快报：英文版 - Tao WEN,Xia ZHAO,Guo An LUO,Jian WANG,Yi Ming WANG,Pan LI,Jun ZHU,Zhong Shang YU,

Fast simultaneous determination of 14 nucleosides and nucleobases in cultured Cordyceps using ultra-performance liquid chromatography - 中国生物学文摘 - Yang,FQ Guan,J Li,SP

Simultaneous Determination of Five Components Including Acetaminophen by Reversed-phase High Performance Liquid Chromatography - 武汉理工大学学报：材料科学英文版 - ZHANGLi-qing,WUXiao-hua,LUYing,WANGXia,

Identification of Novel Pesticides and Impurities by the Combination of LC-MS with GC-MS Analysis - 中国化学：英文版 - 张素艳,耿昱,郭寅龙,王浩,吕龙,

Simultaneous determination of quetiapine and three metabolites in human plasma by high-performance liquid chromatography-electrospray ionization mass spectrometry - 中国药理学报：英文版 - Kun-yanLI Ze-nengCHENG XinLI Xue-lianBAI Bi-kuiZHANG FengWANG Huan-deLI

Simultaneous Separation and Determination of Four Bioactive Constituents in Traditional Chinese Medicinal Tablet Xinkeshu by HPLC-DAD - 中国化学：英文版 - 何建涛石志红闫瑾赵美萍常文保

Micro-Column Separation-ICP-MS Determination of REE Impurities in High-Purity Sm2O3 - 中国稀土学报：英文版 - LiJidong WuXing ZhengYongzhang

Disposable Amperometric Acetylcholinesterase Biosensor for the Detection of Organophosphorus Pesticides - 稀有金属材料与工程 - Xiaohao Wang Xiaowen Xu Fei Tang Zhaoying Zhou

Simultaneous determination of 4-tert-octylphenol, 4-nonylphenol and bisphenol A in Guanting Reservoir using gas chromatography-mass spectrometry with selected ion monitoring - 环境科学学报：英文版 - JINXing-long,HUANGGuo-lan,JIANGGui-bin,ZHOUQun-fang,LIUJmg-fu,

Simultaneous determination of adenine, uridine and adenosine in cordyceps sinensis and its substitutes by LC／ESI-MS - 中南工业大学学报：英文版 - 黄兰芳,吴名剑,孙贤军,郭方遒,梁逸曾,李晓如,

Simultaneous determination of seven impurities in high-purity cobalt oxide by ICP-AES after matrix separation using 1-nitroso-2-naphthol as a precipitant - 中南工业大学学报：英文版 - 王艳,周春山,段青兵,陈萍,

Identification and Determination of Nicorandil and its Degradation Products by HPLC and GC/MS - 中国化学快报：英文版 - Zhong Zhou CHENG,Ze Hui JIA,Yan CHEN,Li Ying CHEN,Hua LI,

Separation of Proteins by Electrophoretic Affinity Chromatography - 中国化学工程学报：英文版 - 邺韶骅刘铮丁富新袁乃驹

【下载文献】

【上一条】：攀钢高炉开铁口机技术进步【下一条】：论英国考克兰锅炉的自动控制特点
[baidu搜索]：Separation of chlorinated hydrocarbons and organophosphorus, pyrethroid pesticides by silicagel fractionation chromatography and their simultaneous determination by GC-MS环境科学学报：英文版论文 [google搜索]：Separation of chlorinated hydrocarbons and organophosphorus, pyrethroid pesticides by silicagel fractionation chromatography and their simultaneous determination by GC-MS环境科学学报：英文版论文